Optimizing dissolution dynamic nuclear polarization.
-
Bornet A
Institut des Sciences et Ingénierie Chimiques, Ecole Polytechnique Fédérale de Lausanne (EPFL), Batochime, CH-1015 Lausanne, Switzerland. Electronic address: aurelien.bornet@epfl.ch.
-
Jannin S
Institut des Sciences et Ingénierie Chimiques, Ecole Polytechnique Fédérale de Lausanne (EPFL), Batochime, CH-1015 Lausanne, Switzerland; Bruker BioSpin AG, Industriestrasse 26, 8117 Fällanden, Switzerland. Electronic address: sami.jannin@epfl.ch.
Published in:
- Journal of magnetic resonance (San Diego, Calif. : 1997). - 2016
English
This article is a short review of some of our recent developments in dissolution dynamic nuclear polarization (d-DNP). We present the basic principles of d-DNP, and motivate our choice to step away from conventional approaches. We then introduce a modified d-DNP recipe that can be summed up as follows. (i) Using broad line polarizing agents to efficiently polarize 1H spins. (ii) Increasing the magnetic field to 6.7 T and above. (iii) Applying microwave frequency modulation. (iv) Applying (1)H-(13)C cross polarization. (v) Transferring hyperpolarized solution through a magnetic tunnel.
-
Language
-
-
Open access status
-
bronze
-
Identifiers
-
-
Persistent URL
-
https://folia.unifr.ch/global/documents/102446
Statistics
Document views: 13
File downloads: